A comparison of three methods used for determining chloride in acid copper sulfate plating bath / Gan Yen Shing

Gan, Yen Shing (2014) A comparison of three methods used for determining chloride in acid copper sulfate plating bath / Gan Yen Shing. Masters thesis, University of Malaya.

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    Abstract

    Monitoring of chloride concentration in acid copper suflate plating bath is vital due to its important role in the quality of copper deposition. In this study, three different analytical methods which include potentiometric titration, UV-Vis spectroscopy and ion chromatography were used to determine the chloride in an actual acid copper sulfate plating bath to investigate their respective analytical performances. From the Oneway Anova and Tukey-Kramer test conducted, it can be concluded that the results from these three methods are significant different, with ion chromatography method showing the greatest difference compared to the other two methods. Besides this, it is determined that potentiometric titration method has an excellent precision and accuracy, UV-Vis method is quite precise but less accurate, and IC method is the least precise and accurate. Taking account of other factors such as skill required, reagents required, sample preparation time, analysis time, cost per sample, maintenance cost and others, potentiometric titration method is the most ideal method to be used.

    Item Type: Thesis (Masters)
    Additional Information: M.Sc. -- Jabatan Kimia, Fakulti Sains, Universiti Malaya, 2014.
    Uncontrolled Keywords: Chloride; Acid copper sulfate plating bath
    Subjects: Q Science > Q Science (General)
    Q Science > QD Chemistry
    Divisions: Faculty of Science
    Depositing User: Mrs Nur Aqilah Paing
    Date Deposited: 05 Mar 2015 14:36
    Last Modified: 05 Mar 2015 14:36
    URI: http://studentsrepo.um.edu.my/id/eprint/4920

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